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Primary Amines on Rtx-35 Amine

ColumnRtx-35 Amine, 30 m, 0.53 mm ID, 1.00 µm (cat.# 11355)
SamplePrimary amines
Diluent:Water
Conc.:50 ppm on-column
Injection
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Splitless taper (4 mm), base deactivated Siltek (cat.# 20798-210.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:35 °C (hold 5 min)
Carrier GasHe, constant pressure
Linear Velocity:35.7 cm/sec
DetectorFID @ 300 °C
NotesSplitless taper (4 mm), base deactivated Siltek Liner obsolete, recommend catalog number 20798.