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Semivolatiles CLP Method on Rtx-5MS

GC_EV00544
PeakstR (min)
1.2-Fluorophenol (SS)4.65
2.Phenol-d6 (SS)5.53
3.Phenol5.55
4.Bis(2-chloroethyl) ether5.64
5.2-Chlorophenol-d4 (SS)5.66
6.2-Chlorophenol5.67
7.1,3-Dichlorobenzene5.81
8.1,4-Dichlorobenzene-d4 (IS)5.86
9.1,4-Dichlorobenzene5.87
10.1,2-Dichlorobenzene-d4 (IS)6.01
11.Benzyl alcohol6.01
12.1,2-Dichlorobenzene6.03
13.2-Methylphenol6.10
14.Bis(2-chloroisopropyl) ether6.13
15.4-Methylphenol/3-Methylphenol6.25
16.N-Nitrosodi-N-propylamine6.28
17.Hexachloroethane6.33
18.Nitrobenzene-d5 (SS)6.41
19.Nitrobenzene6.43
20.Isophorone6.66
21.2-Nitrophenol6.73
22.2,4-Dimethylphenol6.75
23.Bis(2-chloroethoxy)methane6.85
24.Benzoic acid6.91
25.2,4-Dichlorophenol6.95
26.1,2,4-Trichlorobenzene7.03
PeakstR (min)
27.Naphthalene-d8 (IS)7.08
28.Naphthalene7.10
29.4-Chloroaniline7.20
30.Hexachlorobutadiene7.21
31.4-Chloro-3-methylphenol7.62
32.2-Methylnaphthalene7.77
33.Hexachlorocyclopentadiene7.92
34.2,4,6-Trichlorophenol8.05
35.2,4,5-Trichlorophenol8.08
36.2-Fluorobiphenyl (SS)8.13
37.2-Chloronaphthalene8.25
38.2-Nitroaniline8.38
39.Dimethyl phthalate8.54
40.2,6-Dinitrotoluene8.62
41.Acenaphthylene8.66
42.Acenaphthene-d10 (IS)8.79
43.Acenaphthene8.83
44.3-Nitroaniline8.88
45.2,4-Dinitrophenol8.88
46.4-Nitrophenol8.92
47.Dibenzofuran8.99
48.2,4-Dinitrotoluene9.01
49.Diethyl phthalate9.22
50.4-Chlorophenyl phenyl ether9.32
51.Fluorene9.33
52.4-Nitroaniline9.39
PeakstR (min)
53.2-Methyl-4,6-dinitrophenol9.40
54.Diphenylamine9.44
55.2,4,6-Tribromophenol (SS)9.57
56.4-Bromophenyl phenyl ether9.80
57.Hexachlorobenzene9.88
58.Pentachlorophenol10.07
59.Phenanthrene-d10 (IS)10.24
60.Phenanthrene10.27
61.Anthracene10.32
62.Carbazole10.49
63.di-n-Butyl phthalate10.84
64.Fluoranthene11.62
65.Pyrene11.94
66.p-Terphenyl-d14 (SS)12.16
67.Butyl benzyl phthalate13.01
68.Benzo[a]anthracene14.05
69.3,3'-Dichlorobenzidine14.06
70.Chrysene-d12 (IS)14.08
71.Chrysene14.14
72.Bis(2-ethylhexyl)phthalate14.2
73.Di-n-octyl phthalate15.77
74.Benzo[b]fluoranthene16.57
75.Benzo[k]fluoranthene16.64
76.Benzo[a]pyrene17.38
77.Perylene-d12 (IS)17.52
78.Indeno[1,2,3-cd]pyrene20.18
79.Dibenzo[a,h]anthracene20.26
80.Benzo[ghi]perylene20.81
ColumnRtx-5MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 12623)
SampleCLP standard
Conc.:80 ng
Injectionsplitless
Inj. Temp.:300 °C
Oven
Oven Temp.:40 °C (hold 2 min) to 245 °C at 25 °C/min to 330 °C at 6 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.0 mL/min
DetectorMS
Mode:Scan
Source Temp.:280 °C
Scan Range:35-550 amu