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500pg of Derivatized Organo Tin Compounds Separated Well on Rtx-5 and Rtx-35 Columns Using GC/FPD.

GC_EV00787
Peaks
1.Tetrapropyltin
2.Tetrabutyltin
3.Tributyltin
4.Dibutyltin
5.Tripentyltin
6.Monobutyltin
ColumnsRtx-5 30 m, 0.32 mm ID, 1.00 µm (cat.# 10254)
and Rtx-35 30 m, 0.32 mm ID, 1.00 µm (cat.# 10454)
SampleDerivatized Organo Tin Compounds
Conc.:500 pg on column
Injection
Inj. Vol.:3.0 µL Direct
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C (hold 1 min) to 285 °C at 10 °C/min (hold 10 min)
Carrier GasHe, constant pressure (15 psi, 103.4 kPa)
DetectorFPD @ 250 °C