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Minnesota Dept. of Agriculture List 1 Pesticides on Rxi-1ms

ColumnRxi-1ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13323)
SampleMinnesota Ag List 1 Pesticides Mix A (cat.# 32406)
Minnesota Ag List 1 Pesticides Mix B (cat.# 32407)
SV Internal Standard Mix (cat.# 31206)
B/N Surrogate Mix (4/89 SOW) (cat.# 31024)
Acid Surrogate Mix (4/89 SOW) (cat.# 31025)
Conc.:10 µg/mL each analyte (internal standards 25ug/ml)
Injection
Inj. Vol.:1.0 µL split (split ratio 10:1)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:250 °C
Oven
Oven Temp.:70 °C (hold 1 min) to 180 °C at 20 °C/min to 230 °C at 5 °C/min to 325 °C at 40 °C/min (hold 3.5 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Solvent Delay Time:2.5 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD