Welcome to the New Restek.com! Take a tour of the new site and feel free to send us your feedback.
Your web browser will no longer be supported by Restek.com as of 30 June 2021.
To avoid any interruption in access or functionality, install a current-generation web browser now. Learn more.

Semivolatiles on Rxi-5ms by EPA Method 525.2

GC_EV00859
Peaks
1.Isophorone
2.2-Nitro-m-xylene (SS)
3.Naphthalene
4.Dichlorvos (DDVP)
5.Hexachlorocyclopentadiene
6.EPTC
7.Mevinphos
8.Butylate
9.Vernolate
10.Dimethyl phthalate
11.Pebulate
12.Etridiazole
13.2,6-Dinitrotoluene
14.Acenaphthylene
15.Acenaphthene-d10 (IS)
16.Chloroneb
17.Tebuthiuron
18.2,4-Dinitrotoluene
19.Molinate
20.Diethyl phthalate
21.Fluorene
22.Propachlor
23.Ethoprop (ethoprophos)
24.Cycloate
25.Chlorpropham
26.Trifluralin
27.Atraton
28.Hexachlorobenzene
29.Prometon
30.Simazine
31.Atrazine
Peaks
32.Propazine
33.Pentachlorophenol
34.Terbufos
35.Propyzamide
36.Diazinon
37.Phenanthrene-d10 (IS)
38.Phenanthrene
39.Disulfoton
40.Methylparaoxon
41.Anthracene
42.Terbacil
43.Chlorothalonil
44.Metribuzin
45.Simetryn
46.Ametryn
47.Alachlor
48.Prometryn
49.Terbutryn
50.di-n-Butyl phthalate
51.Bromacil
52.Cyanazine (Bladex)
53.Metolachlor
54.Chlorpyrifos
55.Triadimefon
56.DCPA methyl ester (Chlorthal-dimethyl)
57.MGK-264 (isomer A)
58.Diphenamid
59.MGK-264 (isomer B)
60.Merphos
61.Heptachlor epoxide
62.Fluoranthene
Peaks
63.Stirofos
64.Disulfoton sulfone
65.Butachlor
66.Pyrene-d10 (SS)
67.Fenamiphos
68.Pyrene
69.Napropamide (Devrinol)
70.trans-Nonachlor
71.Merphos oxide
72.Tricyclazole (Beam)
73.Carboxin
74.Chlorobenzilate
75.Benzyl butyl phthalate
76.Norflurazon
77.Bis(2-ethylhexyl) adipate
78.Hexazinon (Velpar)
79.Triphenylphosphate (SS)
80.Benz[a]anthracene
81.Chrysene-d12 (IS)
82.Chrysene
83.Bis(2-ethylhexyl) phthalate
84.Fenarimol
85.cis-Permethrin
86.trans-Permethrin
87.Di-n-octyl phthalate
88.Benzo[b]fluoranthene
89.Benzo[k]fluoranthene
90.Benzo[a]pyrene
91.Fluridone (Sonar)
92.Perylene-d12 (SS)
93.Indeno[1,2,3-cd]pyrene
94.Dibenzo[a,h]anthracene
95.Benzo[ghi]perylene
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleMethod 525.2 semivolatile mix (revised) (cat.# 31899)
Organonitrogen pesticide mix #1 (rev), Method 525.2 (cat.# 33012)
Organochlorine pesticide mix #2 (rev), Method 525.2 (cat.# 33011)
Organophosphorus pesticide mix #1 (rev), Method 525.2 (cat.# 33013)
Method 525.2 nitrogen/phosphorus pesticide mix #2 (cat.# 32423)
Method 525.2 internal standard mix (cat.# 31825)
Method 525.2 surrogate standard mix (cat.# 31826)
Conc.:25 µg/mL for each IS and SS, 10 μg/mL each analyte
Injection
Inj. Vol.:1.0 µL pulsed splitless (hold 0.15 min)
Liner:Drilled Uniliner (hole near bottom) (cat.# 20771)
Inj. Temp.:250 °C
Pulse Pressure:50 psi (344.7kPa)
Pulse Time:0.3 min
Purge Flow:80 mL/min
Oven
Oven Temp.:90 °C (hold 1 min) to 270 °C at 20 °C/min to 315 °C at 6 °C/min
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Solvent Delay Time:3.00 min
Tune Type:DFTPP
Ionization Mode:EI
Scan Range:35-550 amu
InstrumentHP6890 GC & 5973 MSD
NotesGas saver is on at 15 mL/min. (1 minute).