Aroclor 1221 PCBs on Rtx-CLPesticides2

	Peaks
1.	Decachlorobiphenyl (DCB)

Injection
Column	Rtx-CLPesticides2, 30 m, 0.32 mm ID, 0.25 µm (cat.# 11324)
Standard/Sample	Aroclor 1221 in hexane diluted to 1,000 ppb
	decachlorobiphenyl (BZ #209) in acetone diluted to 100 ppb (cat.# 32029)
Inj. Vol.:	1.0 µL pulsed splitless (hold 0.3 min)
Liner:	Cyclo Double Gooseneck (4mm) (cat.# 20895)
Inj. Temp.:	250 °C
Pulse Pressure:	30 psi (206.8kPa)
Oven
Oven Temp.:	120 °C to 200 °C at 45 °C/min to 230 °C at 15 °C/min to 330 °C at 30 °C/min (hold 2 min)
Carrier Gas	He, constant linear velocity
Linear Velocity:	60 cm/sec @ 120 °C

Detector	ECD @ 330 °C
Notes	This chromatogram was obtained using an Agilent μ-ECD. To obtain comparable results, you will need to employ a μ-ECD in addition to confirmational dual-columns connected to a 5-meter guard column using a “Y” Press-Tight connector.