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Brominated Flame Retardants on Rtx-1614

GC_EV01019
Peaks
1.BDE-10
2.BDE-7
3.BDE-8
4.BDE-11
5.BDE-12
6.BDE-13
7.BDE-15
8.BDE-30
9.BDE-32
10.BDE-17
11.BDE-25
12.BDE-28
13.BDE-33
Peaks
14.BDE-35
15.BDE-37
16.BDE-75
17.BDE-49
18.BDE-71
19.BDE-47
20.BDE-66
21.BDE-77
22.BDE-100
23.BDE-119
24.BDE-99
25.BDE-116
26.BDE-118
Peaks
27.BDE-85
28.BDE-155
29.BDE-126
30.BDE-154
31.BDE-153
32.BDE-138
33.BDE-166
34.BDE-183
35.BDE-181
36.BDE-190
37.BDE-208
38.BDE-207
39.BDE-206
40.BDE-209
ColumnRtx-1614, 30 m, 0.25 mm ID, 0.10 µm (cat.# 10295)
Sample100-300 ppb PBDE PAR solution (cat.# EO-5113, Cambridge Isotope Laboratories Inc.)
500 ppb decabromodiphenyl ether (cat.# BDE-209, Wellington Laboratories)
Injection
Inj. Vol.:1 µL splitless (hold 1 min)
Liner:Cyclo double taper (4 mm) (cat.# 20896)
Inj. Temp.:300 °C
Oven
Oven Temp.:100 °C (hold 3 min) to 320 °C at 5 °C/min (hold 15 min)
Carrier GasHe, constant linear velocity
Linear Velocity:20 cm/sec @ 100 °C
Detectorµ-ECD @ 340 °C