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Polycyclic Aromatic Hydrocarbons on Rxi-17Sil MS

GC_EV1160
Peaks
1.Naphthalene
2.2-Methylnaphthalene
3.1-Methylnaphthalene
4.Acenaphthylene
5.Acenaphthene
6.Fluorene
7.Phenanthrene
8.Anthracene
9.Fluoranthene
10.Pyrene
11.Benz[a]anthracene
12.Chrysene
13.Triphenylene
Peaks
14.Benzo[b]fluoranthene
15.Benzo[k]fluoranthene
16.Benzo[j]fluoranthene
17.Benzo[a]pyrene
18.3-Methylcholanthrene
19.Dibenz[a,h]acridine
20.Dibenz[a,j]acridine
21.Indeno[1,2,3-cd]pyrene
22.Dibenz[a,h]anthracene
23.Benzo[ghi]perylene
24.7H-Dibenzo[c,g]carbazole
25.Dibenzo[a,e]pyrene
26.Dibenzo[a,i]pyrene
27.Dibenzo[a,h]pyrene
ColumnRxi-17Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 14123)
Standard/SamplePAH Supplement Mix for Method 8100 (cat.# 31857)
EPA Method 8310 PAH mixture (cat.# 31841)
Triphenylene (custom)
Diluent:Dichloromethane
Conc.:10 ppm
Injection
Inj. Vol.:0.5 µL splitless (hold 1.75 min)
Liner:Auto SYS XL PSS split/splitless w/wool (cat.# 21718)
Inj. Temp.:320 °C
Purge Flow:75 mL/min
Oven
Oven Temp.:65 °C (hold 0.5 min) to 220 °C at 15 °C/min to 330 °C at 4 °C/min (hold 15 min)
Carrier GasHe, constant flow
Flow Rate:2.0 mL/min
DetectorFID @ 320 °C
InstrumentPE Clarus 600 GC
AcknowledgementInstrument provided by PerkinElmer
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