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Polycyclic Aromatic Hydrocarbons on Rxi-17Sil MS

ColumnRxi-17Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 14123)
SamplePAH Supplement Mix for Method 8100 (cat.# 31857)
EPA Method 8310 PAH mixture (cat.# 31841)
Triphenylene (custom)
Diluent:Dichloromethane
Conc.:10 ppm
Injection
Inj. Vol.:0.5 µL splitless (hold 1.75 min)
Liner:Auto SYS XL PSS split/splitless w/wool (cat.# 21718)
Inj. Temp.:320 °C
Purge Flow:75 mL/min
Oven
Oven Temp.:65 °C (hold 0.5 min) to 220 °C at 15 °C/min to 330 °C at 4 °C/min (hold 15 min)
Carrier GasHe, constant flow
Flow Rate:2.0 mL/min
DetectorFID @ 320 °C
InstrumentPE Clarus 600 GC
AcknowledgementInstrument provided by PerkinElmer