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Benzofluoranthenes on Rxi-17Sil MS (15m x 0.25mm x 0.25µm)

ColumnRxi-17Sil MS, 15 m, 0.25 mm ID, 0.25 µm (cat.# 14120)
Diluent:Methylene chloride
Conc.:20 ng/µL
Inj. Vol.:1 µL split (split ratio 20:1)
Liner:4 mm split Precision liner w/wool (cat.# 21022)
Inj. Temp.:275 °C
Split Vent Flow Rate:42 mL/min
Oven Temp.:80 °C (hold 1 min) to 320 °C at 15 °C/min (hold 2 min)
Carrier GasH2, constant flow
Flow Rate:2 mL/min
DetectorFID @ 340 °C
Constant Column + Constant Make-up:50 mL/min
Make-up Gas Type:N2
Data Rate:20 Hz
InstrumentAgilent/HP6890 GC