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Diesel Fuel #2 Standard on Rxi-5Sil MS by Split Injection

ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Standard/SampleDiesel fuel #2: unweathered (cat.# 31233)
Diluent:Methylene chloride
Conc.:5000 µg/mL
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Topaz 4 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:300 °C
Oven Temp.:55 °C (hold 0.5 min) to 150 °C at 20 °C/min to 250 °C at 30 °C/min to 280 °C at 5 °C/min to 345 °C at 30 °C/min (hold 3 min)
Carrier GasHe, constant flow
Flow Rate:4 mL/min
DetectorFID @ 340 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:50 Hz
InstrumentAgilent 7890A GC