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|Column||Rxi-5ms, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13424)|
|Sample||No sample injected; instrument ran the method conditions with no injection.|
|Injection||splitless (hold 0.5 min)|
|Liner:||4 mm ID straight inlet liner w/wool, IP deactivated (cat.# 20782)|
|Inj. Temp.:||250 °C|
|Purge Flow:||40 mL/min|
|Oven Temp.:||50 °C (hold 5 min) to 320 °C at 30 °C/min (hold 10 min)|
|Carrier Gas||He, constant flow|
|Flow Rate:||5.0 mL/min|
|Detector||FID @ 330 °C|
|Notes||System was conditioned for 10 min at the following temperatures: inlet 300 °C, oven 310 °C, detector 330 °C.|