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Two Brands of Gin on Stabilwax-MS (Overlay)

GC_FF1237
PeakstR (min)
1.α-Pinene6.16
2.Beta-myrcene10.05
3.D-Limonene10.81
4.Isoamyl alcohol*11.64
5.γ-Terpinene12.08
PeakstR (min)
6.Camphor*17.97
7.Linalool18.56
8.4-Terpineol19.56
9.α-Terpineol*21.18
10.Nerol acetate*22.14
11.Geraniol*23.55
* Not found in gin represented by red trace.
ColumnStabilwax-MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 10673)
SampleTwo different brands of gin
Conc.:Neat
Injection
Inj. Vol.:1 µL split (split ratio 20:1)
Liner:Premium 3.5 mm Precision liner w/wool (cat.# 23320.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:35 °C (hold 5 min) to 250 °C at 7 °C/min (hold 5 min)
Carrier GasHe, constant linear velocity
Linear Velocity:36 cm/sec
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
10.540-5502
Transfer Line Temp.:260 °C
Analyzer Type:Quadrupole
Source Temp.:250 °C
Solvent Delay Time:0.5 min
Ionization Mode:EI
InstrumentShimadzu 2010 GC & QP2010+ MS