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Citronella Java Oil on Rtx-Wax

GC_FF1296
PeakstR (min)
1.D-Limonene1.809
2.Citronellal2.092
3.Linalool3.184
4.Isopulegol3.397
5.γ-Elemene3.561
6.β-Caryophyllene3.638
7.Citronellyl propionate3.917
8.α-Terpineol4.029
PeakstR (min)
9.Germacrene D4.290
10.Geranyl acetate4.509
11.β-Citronellol4.509
12.δ-Cadinene4.569
13.Nerol4.722
14.Geraniol5.006
15.α-Elemol6.417
16.Eugenol6.884
ColumnRtx-Wax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 12424)
SampleCitronella java oil
Diluent:Acetone
Conc.:5%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:230 °C
Oven
Oven Temp.:100 °C (hold 0.5 min) to 250 °C at 16 °C/min (hold 10 min)
Carrier GasH2, constant flow
Flow Rate:2 mL/min
DetectorFID @ 250 °C
Constant Column + Constant Make-up:52 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:400 mL/min
Data Rate:50 Hz
InstrumentAgilent 7890A GC
NotesAll peaks were identified using the NIST MS EI spectra library (2005).