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Peaks | tR (min) | |
---|---|---|
1. | α-Pinene | 1.473 |
2. | Camphene | 1.544 |
3. | β-Pinene | 1.617 |
4. | β-Myrcene | 1.68 |
5. | Limonene | 1.807 |
6. | Eucalyptol | 1.844 |
Peaks | tR (min) | |
---|---|---|
7. | γ-Terpinene | 1.933 |
8. | p-Cymene | 2.015 |
9. | Camphor | 3.158 |
10. | Caryophyllene | 3.637 |
11. | α-Terpineol | 4.098 |
12. | Borneol | 4.148 |
Column | Rtx-Wax, 30 m, 0.32 mm ID, 0.25 µm (cat.# 12424) |
---|---|
Standard/Sample | Rosemary oil |
Diluent: | Acetone |
Conc.: | 5% |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 100:1) |
Liner: | Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305) |
Inj. Temp.: | 230 °C |
Oven | |
Oven Temp.: | 100 °C (hold 0.5 min) to 250 °C at 16 °C/min (hold 10 min) |
Carrier Gas | H2, constant flow |
Flow Rate: | 2 mL/min |
Detector | FID @ 250 °C |
---|---|
Constant Column + Constant Make-up: | 52 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 400 mL/min |
Data Rate: | 50 Hz |
Instrument | Agilent 7890A GC |
Notes | All peaks were identified using the NIST MS EI spectra library (2005). |