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Patchouli Oil on Rxi-5Sil MS

GC_FF1312
PeakstR (min)
1.α-Pinene2.062
2.β-Pinene2.290
3.D-Limonene2.545
4.δ-Elemene5.246
5.β-Elemene5.829
6.β-Patchoulene5.867
7.Caryophyllene6.222
8.α-Guaiene6.344
PeakstR (min)
9.Seychellene6.596
10.α-Patchoulene6.710
11.β-Guaiene6.741
12.Patchoulene6.795
13.Cedrene6.991
14.δ-Guaiene7.069
15.Valencene8.691
16.Patchoulol8.937
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
SamplePatchouli oil
Diluent:Acetone
Conc.:5%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 300 °C at 11 °C/min (hold 10 min)
Carrier GasHe, constant flow
Flow Rate:1.31 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
11.0035-5005
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Type:Inert
Source Temp.:230 °C
Quad Temp.:150 °C
InstrumentAgilent 7890A GC & 5975C MSD
NotesAll peaks were identified using the NIST MS EI spectra library (2005).