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Tea Tree Oil on Rxi-5Sil MS

GC_FF1317
PeakstR (min)
1.α-Pinene2.067
2.Terpinolene2.474
3.p-Cymene2.516
4.D-Limonene2.552
5.Eucalyptol2.591
6.γ-Terpinene2.731
7.Pinocarveol3.424
8.Terpinen-4-ol3.756
PeakstR (min)
9.α-Terpineol3.849
10.Nerol4.046
11.Geraniol4.265
12.γ-Elemene5.228
13.Caryophyllene6.217
14.Aromadendrene6.415
15.α-Caryophyllene6.587
16.Alloaromadendrene6.642
17.Ledene6.947
ColumnRxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
SampleTea tree oil
Diluent:Acetone
Conc.:5%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 300 °C at 11 °C/min (hold 10 min)
Carrier GasHe, constant flow
Flow Rate:1.31 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
11.0035-5005
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Type:Inert
Source Temp.:230 °C
Quad Temp.:150 °C
InstrumentAgilent 7890A GC & 5975C MSD
NotesAll peaks were identified using the NIST MS EI spectra library (2005).