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Lavender Oil on Rxi-5Sil MS (10 m, 0.15 mm ID, 0.15 µm)

GC_FF1337
PeakstR (min)
1.α-Thujene0.499
2.α-Pinene0.513
3.Camphene0.535
4.1-Octen-3-ol0.544
5.β-Phellandrene0.559
6.β-Pinene0.567
7.Hexyl acetate0.579
8.β-Ocimene0.621
9.D-Limonene0.630
10.Eucalyptol0.640
11.γ-Terpinene0.670
12.Linalool oxide0.693
13.Terpinolene0.715
PeakstR (min)
14.Linalool0.736
15.Camphor0.855
16.Borneol0.902
17.4-Carvomenthenol0.915
18.α-Terpineol0.941
19.Linalyl acetate1.050
20.Lavandulyl acetate1.117
21.Neryl acetate1.304
22.Geranyl acetate1.354
23.Caryophyllene1.514
24.β-Farnesene1.558
25.β-Cubebene1.667
26.α-Bisabolol2.163
ColumnRxi-5Sil MS, 10 m, 0.15 mm ID, 0.15 µm (cat.# 43815)
SampleLavender oil
Diluent:Acetone
Conc.:1%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:250 °C
Oven
Oven Temp.:100 °C to 300 °C at 45 °C/min to 320 °C at 30 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.01 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
11.0035-50011
Transfer Line Temp.:300 °C
Analyzer Type:Quadrupole
Source Type:Inert
Source Temp.:230 °C
Quad Temp.:150 °C
InstrumentAgilent 7890A GC & 5975C MSD
NotesAll peaks were identified using the NIST MS EI spectra library (2005).