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GC Multiresidue Pesticide Standard #3-ONP on Rxi-5ms by GC-MS

GC_FS0602
PeakstR (min)
1.2,6-Dichlorobenzonitrile (Dichlobenil)7.72
2.Biphenyl8.24
3.3,4'-Dichloroaniline8.95
4.THPI (Tetrahydrophthalimide)9.64
5.Tetrachloronitrobenzene (Tecnazene)11.42
6.Diphenylamine11.63
7.2,3,5,6-Tetrachloroaniline11.70
8.Ethalfluralin12.18
9.Trifluralin12.40
10.Benfluralin12.45
11.Dicloran12.99
12.Pentachloronitrobenzene (Quintozene)13.65
PeakstR (min)
13.Pentachlorobenzonitrile13.69
14.Profluralin13.76
15.Fluchloralin14.06
16.Chlorothalonil14.21
17.Pentachloroaniline14.64
18.Prodiamine15.78
19.Dichlofluanid15.90
20.Isopropalin16.77
21.Pendimethalin16.95
22.Tolylfluanid17.07
23.Oxyfluorfen18.51
24.Nitrofen18.77
25.Nitralin20.69
ColumnRxi-5ms, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13423)
SampleGC multiresidue pesticide standard #3-ONP (cat.# 32565)
Diluent:Toluene
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Premium 4.0 mm ID Precision inlet liner w/wool (cat.# 23305.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:90 °C (hold 1 min) to 330 °C at 8.5 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:1.4 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1555-5507
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Electron Energy:70 eV
Solvent Delay Time:5 min
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesReconstructed chromatogram from select ions.