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Cannabis Terpenes Standard #1 & #2 on Rxi-624Sil MS

GC_GN1200
PeakstR (min)
1.alpha-Pinene5.399
2.Camphene5.768
3.beta-Myrcene6.203
4.(-)-beta-Pinene6.290
5.delta-3-Carene6.816
6.alpha-Terpinene7.026
7.Ocimene 17.158
8.D-Limonene7.281
9.p-Cymene7.362
10.Ocimene 27.539
11.Eucalyptol7.629
PeakstR (min)
12.Gamma terpinene7.990
13.Terpinolene8.887
14.Linalool9.845
15.(-)-Isopulegol10.874
16.Geraniol11.991
17.beta-Caryophyllene13.303
18.alpha-Humulene13.531
19.Nerolidol 113.855
20.Nerolidol 214.012
21.(-)-Guaiol14.393
22.Caryophyllene oxide14.483
23.(-)-alpha-Bisabolol14.747
ColumnRxi-624Sil MS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 13868)
SampleCannabis terpenes standard #1 (cat.# 34095)
Cannabis terpenes standard #2 (cat.# 34096)
Diluent:Isopropanol
Conc.:25 µg/mL (5 μg/mL on-column after 5:1 split)
Injection
Inj. Vol.:1 µL split (split ratio 5:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:250 °C
Split Vent Flow Rate:6 mL/min
Oven
Oven Temp.:55 °C to 130 °C at 25 °C/min (hold 6 min) to 280 °C at 30 °C/min (hold 2 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)
Scan Range
(amu)
Scan Rate
(scans/sec)
1535-2805.6
Transfer Line Temp.:310 °C
Analyzer Type:Quadrupole
Source Type:Inert
Drawout Plate:6 mm ID
Source Temp.:330 °C
Quad Temp.:180 °C
Solvent Delay Time:5 min
Tune Type:PFTBA
Ionization Mode:EI
InstrumentAgilent 7890A GC & 5975C MSD
Notes