Cannabis Terpenes Standard #1 & #2 on Rxi-624Sil MS

Injection
Column	Rxi-624Sil MS, 30 m, 0.25 mm ID, 1.40 µm (cat.# 13868)
Standard/Sample	Cannabis terpenes standard #1 (cat.# 34095)
	Cannabis terpenes standard #2 (cat.# 34096)
Diluent:	Isopropanol
Conc.:	25 µg/mL (5 μg/mL on-column after 5:1 split)
Inj. Vol.:	1 µL split (split ratio 5:1)
Liner:	Topaz 4.0 mm ID Precision inlet liner w/wool (cat.# 23305)
Inj. Temp.:	250 °C
Split Vent Flow Rate:	6 mL/min
Oven
Oven Temp.:	55 °C to 130 °C at 25 °C/min (hold 6 min) to 280 °C at 30 °C/min (hold 2 min)
Carrier Gas	He, constant flow
Flow Rate:	1.2 mL/min

Detector

Mode:

Scan

Scan Program:

Group	Start Time (min)	Scan Range (amu)	Scan Rate (scans/sec)
1	5	35-280	5.6

Transfer Line Temp.:

310 °C

Analyzer Type:

Quadrupole

Source Type:

Inert

Drawout Plate:

6 mm ID

Source Temp.:

330 °C

Quad Temp.:

180 °C

Solvent Delay Time:

5 min

Tune Type:

PFTBA

Ionization Mode:

Instrument

Agilent 7890A GC & 5975C MSD

Notes

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