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ASTM D6584 Derivatized B100 and Internal Standards on MXT-Biodiesel TG

GC_PC00935
ColumnMXT-Biodiesel TG w/2 m x 0.53 mm retention gap, 10 m, 0.32 mm ID, 0.10 µm (cat.# 70290)
SampleB100 + IS butanetriol & tricaprin derivatized with MSTFA as per ASTM D6584
Injection
Inj. Vol.:1.0 µL cold on-column
Temp. Program:Oven track
Oven
Oven Temp.:50 °C (hold 1 min) to 180 °C at 15 °C/min to 230 °C at 7 °C/min to 430 °C at 30 °C/min (hold 5 min)
Carrier GasH2, constant flow
Flow Rate:4 mL/min
DetectorFID @ 430 °C