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Impurities in Methyl-t-Butyl Ether (MTBE) on Rtx-DHA-150 (ASTM D5441)

ColumnRtx-DHA-150, 150 m, 0.25 mm ID, 1.00 µm (cat.# 10149)
SampleASTM D5441 MTBE contaminants mix
Conc.:1 % (w/w) each component in MTBE
Injection
Inj. Vol.:0.2 µL split (split ratio 200:1)
Liner:Cup splitter (cat.# 20710)
Inj. Temp.:200 °C
Oven
Oven Temp.:60 °C (hold 13 min) to 180 °C at 10 °C/min (hold 20 min)
Carrier GasHe, constant flow
Flow Rate:2.2 mL/min
Linear Velocity:23 cm/sec @ 60 °C
DetectorFID @ 250 °C
Make-up Gas Flow Rate:24 mL/min
Make-up Gas Type:H2
Hydrogen flow:30 mL/min
Air flow:358 mL/min
InstrumentAgilent 7890B GC
NotesResolution between trans-2-pentene/tert-butanol and tert-butanol/cis-2-pentene meets the ASTM Method D5441 requirement of R ≥ 1.3.