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Peaks | |
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1. | Acetic acid |
2. | Formic acid |
3. | Propionic acid |
4. | Isobutyric acid |
5. | n-Butyric acid |
6. | Isovaleric acid |
7. | n-Valeric acid |
8. | Isocaproic acid |
9. | n-Caproic acid |
10. | Heptanoic acid |
Column | 10% FFAP, 1% H3PO4, 100/120 mesh on DiatoSorb-WHP, SilcoSmooth tubing, 2 m, 1/8 in OD, 2 mm ID |
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Standard/Sample | Fatty acids C1-C7 |
Diluent: | Ether |
Conc.: | 1,000 µg/mL |
Injection | |
Inj. Vol.: | 8 µL on-column |
Inj. Temp.: | 200 °C |
Oven | |
Oven Temp.: | 125 °C (hold 2 min) to 175 °C at 10 °C/min (hold 5 min) |
Carrier Gas | He, constant flow |
Flow Rate: | 30 mL/min |
Detector | TCD @ 230 °C |
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Instrument | Agilent 7890B GC |