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Refinery Gas on Rt-Q-BOND

GC_PC1342
PeaksMol%
1.NitrogenBalance
2.Carbon monoxide1.00
3.Methane5.00
4.Carbon dioxide3.00
5.Ethylene2.00
6.Acetylene1.00
7.Ethane4.00
8.Propylene3.00
9.Propane6.00
10.Propadiene1.00
11.Cyclopropane0.04
12.Isobutane5.00
PeaksMol%
13.Isobutene1.00
14.Butene-12.00
15.1,3-Butadiene3.00
16.Butane4.00
17.trans-2-Butene3.00
18.cis-2-Butene2.00
19.Isopentane1.00
20.Pentene-10.40
21.trans-2-Pentene0.40
22.2-Methyl-2-butene0.20
23.Pentane1.00
24.cis-2-Pentene0.15
25.Hexane0.10
ColumnRt-Q-BOND, 30 m, 0.53 mm ID, 20 µm (cat.# 19742)
SampleRefinery gas standard #2 (cat.# 34442)
Injectionsplit
Liner:Topaz 2.0 mm ID straight inlet liner (cat.# 23313)
Inj. Temp.:200 °C
Oven
Oven Temp.:40 °C to 250 °C at 10 °C/min
Carrier GasHe, constant flow
Flow Rate:4 mL/min
DetectorFID
InstrumentAgilent 7890B GC
NotesThe sample was analyzed using two detectors:
1. FID at 260 °C, 40 µL split injection (split ratio 10:1)
2. TCD at 250°C, 150 µL split injection (split ratio 10:1)