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Aliphatic Amines on Stabilwax-DB

GC_PC1361
PeakstR (min)
1.Trimethylamine1.576
2.Dimethylamine1.683
3.Methylamine1.684
4.Ethylamine1.796
5.Isopropylamine1.838
6.Diethylamine1.936
7.Triethylamine1.999
8.Diisopropylamine2.000
9.n-Butylamine2.628
ColumnStabilwax-DB, 30 m, 0.53 mm ID, 1.00 µm (cat.# 10855)
SampleCustom aliphatic amines
Diluent:Methanol
Conc.:1000 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 50:1)
Liner:Topaz 4.0 mm ID single taper inlet liner w/wool (cat.# 23303)
Inj. Temp.:220 °C
Oven
Oven Temp.:45 °C (hold 1 min) to 220 °C at 35 °C/min (hold 5 min)
Carrier GasH2, constant flow
Linear Velocity:40 cm/sec @ 45 °C
DetectorFID @ 220 °C
Make-up Gas Flow Rate:45 mL/min
Make-up Gas Type:N2
Hydrogen flow:40 mL/min
Air flow:450 mL/min
Data Rate:50 Hz
InstrumentAgilent/HP6890 GC