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Noble and Permanent Gases on ShinCarbon

GC_PC1363
Peaks
1.Helium
2.Neon
3.Hydrogen
4.Oxygen
5.Argon
6.Nitrogen
Peaks
7.Carbon monoxide
8.Methane
9.Krypton
10.Carbon dioxide
11.Xenon
12.Sulfur hexafluoride
Column100/120 mesh, ShinCarbon ST micropacked column, 2 m, 1.00 mm ID (cat.# 19808)
SampleNoble and permanent gas standard
Conc.:2-10 mol%
Injection
Inj. Vol.:200 µL split (split ratio 10:1)
Liner:Topaz 2.0 mm ID straight inlet liner (cat.# 23313)
Inj. Temp.:150 °C
Oven
Oven Temp.:35 °C (hold 3 min) to 80 °C at 10 °C/min to 200 °C at 30 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:6.5 mL/min
DetectorTCD @ 250 °C
InstrumentAgilent 7890B GC
NotesChromatogram A Analysis Conditions:
Inj. Vol.: 50 µL, split (split ratio 10:1)
Conc.: 33 mol% each
Inj. Temp.: 150 °C
Oven Temp.: 35 °C isothermal
Carrier Gas: N2, constant flow
Flow Rate: 5.5 mL/min
Detector: TCD @ 250 °C