1-Hexene on Rxi-LAO (60 m x 0.25 mm x 1.4 µm)

Injection
Column	Rxi-LAO, 60 m, 0.25 mm ID, 1.4 µm (cat.# 13876)
Standard/Sample	1-Hexene

Conc.:	Neat solvent
Inj. Vol.:	1 µL split (split ratio 100:1)
Liner:	Topaz 4.0 mm ID low pressure drop Precision inlet liner w/wool (cat.# 23309)
Inj. Temp.:	250 °C
Split Vent Flow Rate:	125 mL/min
Oven
Oven Temp.:	35 °C (hold 20 min) to 160 °C at 30 °C/min (hold 20 min)
Carrier Gas	He, constant flow
Linear Velocity:	23 cm/sec @ 35 °C

Detector	FID @ 300 °C
Make-up Gas Flow Rate:	45 mL/min
Make-up Gas Type:	N₂
Hydrogen flow:	40 mL/min
Air flow:	450 mL/min
Data Rate:	20 Hz
Instrument	Agilent 7890B GC
Sample Preparation	The sample was pipetted into a 2 mL vial (cat.# 21142) and capped with a short screw cap (cat.# 24498).
Notes	• Compounds were tentatively identified using a mass spectrometer and method translation. • A 208V instrument was used. • Benzene is not present in the sample, but if it were, it would elute at 23.73 minutes under these conditions.

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