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Inertness Comparison (Basic Compounds): Primary, Secondary, and Tertiary Amines on Rxi-624Sil MS

GC_PH1162
PeaksConc.
(µg/mL)
1.Isopropylamine100
2.Diethylamine100
3.Triethylamine100
ColumnRxi-624Sil MS, 30 m, 0.32 mm ID, 1.8 µm (cat.# 13870)
Sample
Diluent:DMSO
Conc.:100 µg/mL
Injection
Inj. Vol.:1 µL split (split ratio 20:1)
Liner:5 mm Single taper with wool (cat.# 22973-200.1)
Inj. Temp.:250 °C
Oven
Oven Temp.:50 °C (hold 1 min) to 200 °C at 20 °C/min (hold 5 min)
Carrier GasHe, constant flow
Linear Velocity:37 cm/sec
DetectorFID @ 250 °C
InstrumentAgilent/HP6890 GC