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Synthetic Cannabinoids in Urine on Raptor Biphenyl by LC-MS/MS

LC_CF0584
PeakstR (min)Q1Q3 QuantifierQ3 Qualifier
1.Pravadoline2.11379.29135.04114.16
2.AM22332.38459.25112.2098.15
3.JWH-200-d5 (IS)2.43390.34155.07-
4.JWH-2002.45385.28155.07114.16
5.WIN 55, 2123.41427.29155.07127.14
6.RCS-44.16322.27135.1277.09
7.JWH-015-d7 (IS)4.27335.28155.07-
8.JWH-2504.27336.28121.1291.07
9.JWH-0154.29328.26155.07127.13
PeakstR (min)Q1Q3 QuantifierQ3 Qualifier
10.AM22014.30360.26155.07127.14
11.JWH-2034.39340.23188.18125.09
12.JWH-0734.42328.26155.07127.13
13.JWH-018-d9 (IS)4.55351.34155.07-
14.JWH-0184.57342.27155.08127.11
15.JWH-0814.64372.28185.12157.09
16.JWH-1224.69356.29169.12141.11
17.JWH-0194.70356.29155.07127.10
18.JWH-2104.84370.31183.12153.26
ColumnRaptor Biphenyl (cat.# 9309A5E)
Dimensions:50 mm x 3.0 mm ID
Particle Size:2.7 µm
Guard Column:Raptor Biphenyl EXP 5 mm, 3.0 mm ID, 2.7 µm (cat.# 9309A0253)
Temp.:30 °C
SampleCustom
Conc.: A 5 ng/mL standard was prepared in urine. 1 mL of the 5 ng/mL urine standard was diluted with 2 mL of 0.1% formic acid in 50:50 water:methanol prior to analysis.
Inj. Vol.:2 µL
Mobile Phase
A:0.1% Formic acid in water
B:0.1% Formic acid in acetonitrile
Time (min)Flow (mL/min)%A%B
0.000.6007525
1.00.6007525
5.00.600595
5.50.600595
5.510.6007525
7.00.6007525
DetectorWaters Xevo TQ-S
Ion Source:Waters Zspray™ ESI
Ion Mode:ESI+
Mode:MRM
InstrumentWaters
NotesChromatogram collected using scheduled MRMs.