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Synthetic Cannabinoids in Urine by LC-MS/MS on Raptor Biphenyl

LC_CF0612
PeakstR (min)Precursor IonQuantifier Product Ion Qualifier Product
1.Pravadoline2.15379.29135.04114.16
2.AM22332.44459.25112.298.15
3.JWH-200-d52.47390.34155.07NA
4.JWH-2002.48385.28155.07114.16
5.WIN 55, 2123.34427.29155.07127.14
6.RCS-44.15322.27135.1277.09
7.XLR-114.21330.25232.17125.1
8.JWH-015-d74.27335.28155.07NA
9.JWH-2504.27336.28121.1291.07
10.JWH-0154.29328.26155.07127.13
PeakstR (min)Precursor IonQuantifier Product Ion Qualifier Product
11.AM22014.30360.26155.07127.14
12.JWH-2034.39340.23188.18125.09
13.JWH-0734.42328.26155.07127.13
14.UR-1444.44312.32214.17125.1
15.JWH-018-d94.55351.34155.07NA
16.JWH-0184.57342.27155.08127.11
17.JWH-0814.64372.28185.12157.09
18.JWH-1224.69356.29169.12141.11
19.JWH-0194.70356.29155.07127.1
20.JWH-2104.84370.31183.12153.26
ColumnRaptor Biphenyl (cat.# 9309A5E)
Dimensions:50 mm x 3.0 mm ID
Particle Size:2.7 µm
Guard Column:Raptor Biphenyl EXP guard column cartridge 5.0 mm, 3.0 mm ID, 2.7 µm (cat.# 9309A0253)
Standard/Sample
Conc.:5 ng/mL standard was prepared in urine and diluted 3x with 50:50 methanol:water
Inj. Vol.:2 µL
Mobile Phase
A:0.1% Formic acid in water
B:0.1% Formic acid in acetonitrile
Time (min)Flow (mL/min)%A%B
0.000.67525
1.000.67525
5.000.6595
5.500.6595
5.510.67525
7.000.67525
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentUHPLC