Welcome to the New Restek.com! Take a tour of the new site and feel free to send us your feedback.
Your web browser will no longer be supported by Restek.com as of 30 June 2021.
To avoid any interruption in access or functionality, install a current-generation web browser now. Learn more.

Combined Analysis of Synthetic Cannabinoids & Metabolites in Urine by LC-MS/MS on Raptor Biphenyl

LC_CF0613
PeakstR (min)Precursor IonQuantifier Product Ion Qualifier Product Ion
1.Pravadoline2.15379.29135.04114.16
2.AM22332.44459.25112.298.15
3.JWH-200-d52.47390.34155.07NA
4.JWH-2002.48385.28155.07114.16
5.WIN 55, 2123.34427.29155.07127.14
6.JWH-073 N-butanoic acid3.39358.27155.08127.11
7.JWH-073 4-hydroxybutyl3.4344.24155.09127.09
8.JWH-018 N-pentanoic acid3.49372.18155.08127.14
9.JWH-018 5-hydroxypentyl-d53.54363.5155.08NA
10.JWH-018 5-hydroxypentyl3.55358.27155.08127.11
11.JWH-073 6-hydroxyindole3.77344.24155.09127.09
12.JWH-073 5-hydroxyindole-d73.81351.21155.07NA
13.JWH-073 5-hydroxyindole3.83344.24155.09127.09
14.JWH-073 7-hydroxyindole3.92344.24155.09127.09
15.JWH-018 6-hydroxyindole3.94358.27155.08127.11
16.JWH-018 5-hydroxyindole3.99358.27155.08127.11
17.JWH-018 7-hydroxyindole4.08358.27155.08127.11
PeakstR (min)Precursor IonQuantifier Product Ion Qualifier Product Ion
18.RCS-44.15322.27135.1277.09
19.XLR-114.21330.25232.17125.1
20.JWH-015-d74.27335.28155.07NA
21.JWH-2504.27336.28121.1291.07
22.JWH-0154.29328.26155.07127.13
23.AM22014.30360.26155.07127.14
24.JWH-2034.39340.23188.18125.09
25.JWH-0734.42328.26155.07127.13
26.UR-1444.44312.32214.17125.1
27.JWH-073 4-hydroxyindole4.53344.24155.09127.09
28.JWH-018-d94.55351.34155.07NA
29.JWH-0184.57342.27155.08127.11
30.JWH-0814.64372.28185.12157.09
31.JWH-018 4-hydroxyindole4.66358.27155.08127.11
32.JWH-1224.69356.29169.12141.11
33.JWH-0194.70356.29155.07127.1
34.JWH-2104.84370.31183.12153.26
ColumnRaptor Biphenyl (cat.# 9309A5E)
Dimensions:50 mm x 3.0 mm ID
Particle Size:2.7 µm
Guard Column:Raptor Biphenyl EXP guard column cartridge 5.0 mm, 3.0 mm ID, 2.7 µm (cat.# 9309A0253)
Sample
Conc.:5 ng/mL standard was prepared in urine and diluted 3x with 50:50 methanol:water
Inj. Vol.:2 µL
Mobile Phase
A:0.1% Formic acid in water
B:0.1% Formic acid in acetonitrile
Time (min)Flow (mL/min)%A%B
0.000.67525
1.000.67525
5.000.6595
5.500.6595
5.510.67525
7.000.67525
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentUHPLC