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Carbamate Pesticides on Ultra Carbamate by LC-MS/MS

LC_EV0534
PeakstR (min)Precursor IonProduct IonProduct Ion
1.Aldicarb sulfone1.77240.186.2148.2
2.Aldicarb sulfoxide1.92207.1132.189.1
3.Oxamyl2.01237.172.190.1
4.Methomyl2.22163.1106.088.1
5.3-Hydroxycarbofuran2.68238.1163.0181.0
6.Aldicarb3.44208.1116.089.0
7.Propoxur3.71210.1111.0168.1
8.Carbofuran3.80222.1165.1123.0
9.Carbaryl4.07202.1145.0127.0
10.Methiocarb4.78226.1169.1121.1
ColumnUltra Carbamate (cat.# 9177312)
Dimensions:100 mm x 2.1 mm ID
Particle Size:3 µm
Pore Size:100 Å
Temp.:30 °C
Sample531.1 Carbamate pesticide calibration mixture (cat.# 32273)
Diluent:Water
Conc.:10 ng/mL
Inj. Vol.:5 µL
Mobile Phase
A:0.1% Formic acid + 5 mM ammonium formate in water
B:0.1% Formic acid + 5 mM ammonium formate in methanol
Time (min)Flow (mL/min)%A%B
0.000.57525
5.000.5595
5.010.57525
8.000.57525
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentHPLC