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EU 15+1 PAHs on Pinnacle II PAH (FLD)

ColumnPinnacle II PAH, custom (cat.# 921946E)
Dimensions:150 mm x 3.0 mm ID
Particle Size:4 µm
Pore Size:110 Å
Temp.:30 °C
Samplecustom EU 15+1 PAH mix
Diluent:acetonitrile
Conc.:30 ng/mL (ppb)
Inj. Vol.:5 µL
Mobile Phase
A:water
B:95:5 acetonitrile:tetrahydrofuran
Time (min)Flow (mL/min)%A%B
0.001.53070
3.001.52575
10.001.50100
14.501.50100
14.511.53070
16.501.53070
Max Pressure:275 bar
DetectorShimadzu RF-10AXL
Time (min)Wavelength Ex (nm)Wavelength Em (nm)Gain
02703901x
4.853005124x
5.802904301x
8.403704604x
8.902904301x
9.603704601x
InstrumentShimadzu Prominence
NotesRF-10AXL sensitivity: medium
Cyclopenta(c,d)pyrene was included in the EU 15+1 PAH mix but it does not fluoresce.