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200+ Pesticides in Strawberry on Low-Pressure GC Column Kit

GC_FS0572
PeakstR (min)Precursor IonProduct IonCollision EnergyConfirmation Precursor IonConfirmation Product IonCollision Energy
1.Allidochlor3.37138818132566
2.Dichlobenil3.6317110025136100.110
3.Biphenyl3.75154.111525152.1126.123
4.Mevinphos3.88192127.110127.19516
5.3,4-Dichloroaniline3.921639016161126.18
6.Pebulate4.012031288128578
7.Etridiazole4.02211139.922182.8139.916
8.N-(2,4-Dimethylphenyl) formamide4.1012110681207715
9.Tetrahydrophthalimide4.10151.180.16151.112210
10.Methacrifos4.1924018010125796
11.Chloroneb4.242061911019111313
12.2-Phenylphenol4.31170.2141.222141115.112
13.Pentachlorobenzene4.332501423025017930
14.Propachlor4.601765781207719
15.Tecnazene4.60260.9202.913214.9178.98
16.Diphenylamine4.63169.1167.125169.1168.112
17.Cycloate4.672151546154838
18.2,3,5,6-Tetrachloroaniline4.692311223023116022
19.Chlorpropham4.70213.1171.18171127.18
20.Ethalfluralin4.75316.1276.110276.1202.115
21.Trifluralin4.78306.1206.212306.1264.18
22.Benfluralin4.80292160.120292264.18
23.Sulfotep4.853221462320214610
24.Diallate 14.89234.115018234.1192.112
25.Phorate4.90260.1758121.16510
26.Diallate 24.95234.115018234.1192.112
27.α-BHC5.00219183818114515
28.Hexachlorobenzene5.02283.8213.930248.9213.914
29.Dicloran5.03206147.91817614810
30.Pentachloroanisole5.04279.9236.923266.9238.910
31.Atrazine5.05215173.18200.1122.110
32.Clomazone5.10204107181258913
33.β-BHC5.12219183818114515
34.Profluralin5.14330.16925318.119917
35.Terbuthylazine5.16229.1173.18172.8137.98
36.Terbufos5.172311292323117512
37.γ-BHC5.16219183818114515
38.Propyzamide5.181731092717314513
39.Diazinon5.19304179.112137.184.112
40.Fonofos5.19246.1137.18137.11096
41.Quintozene5.19294.823715236.811922
42.Fluchloralin5.21306.1159.720306.12648
43.Pentachlorobenzonitrile5.212752053027323817
44.Pyrimethanil5.21198.1118.132198.118316
45.Tefluthrin5.24177127.115177137.115
46.Disulfoton5.25153.1971288.159.96
47.Terbacil5.26161144141601178
48.Isazophos5.29172.113010161.11198
49.δ-BHC5.31219183818114515
50.Triallate5.322701861826818420
51.Chlorothalonil5.342661702326416823
52.Anthracene (IS)5.3517815220
53.Endosulfan ether5.42240.920613238.920413
54.Propanil5.4421916382171618
55.Pentachloroaniline5.452651942226319220
56.Dimethachlor5.46197148813410513
57.Acetochlor5.482231322017414612
58.Transfluthrin5.4816314313127.191.18
59.Vinclozolin5.502852121221217212
60.Chlorpyrifos methyl5.522869322286207.912
61.Methyl parathion5.5226310910263136.28
62.Tolclofos-methyl5.542672521026525010
63.Alachlor5.55188160101461188
64.Metalaxyl5.56220.1160.210160.1145.110
65.Propisochlor5.562231321816212013
66.Fenchlorphos5.592872721128524023
67.Heptachlor5.59272237131006512
68.Prodiamine5.6332127962792038
69.Pirimiphos methyl5.65305.1180.18290.112522
70.Fenitrothion5.662771091626012512
71.Linuron5.6924861818712421
72.Malathion5.691739913127996
73.Dichlofluanid5.722241231212377.116
74.Pentachlorothioanisole5.732962463229626312
75.Metolachlor5.762381621016213313
76.Chlorpyrifos5.77314257.912196.9168.914
77.Fenthion5.772781091827816917
78.Parathion5.78291.2109.110109818
79.Anthraquinone5.79208.1180.110180.1152.112
80.Triadimefon5.79208110.924208180.810
81.Aldrin5.80298263826319331
82.Chlorthal-dimethyl5.81331.83018298.9220.924
83.4,4'-Dichlorobenzophenone5.81139752711175.112
84.Pirimiphos ethyl5.85318.2166.112304.1168.112
85.Fenson5.8626877.11814177.18
86.Cyprodinil5.87225.2209.812224.1208.120
87.Diphenamid5.88239167816711540
88.Isopropalin5.89280.1118.125280.1238.18
89.MGK 264 15.89164.18024164.193.112
90.Bromophos-methyl5.903313161332931413
91.Chlozolinate5.95331259.1818614516
92.Pendimethalin5.95281.1252.28252.1162.110
93.Bioallethrin5.96136.19311123.281.18
94.Fipronil5.973672133036921530
95.MGK 264 25.971646710164.18024
96.Isodrin5.97260.9190.92819312330
97.Metazachlor5.972091321513311725
98.Penconazole5.97248.1192161598930
99.Chlorfenvinphos 16.043232671026715915
100.Tolylfluanid6.052401371023813710
101.Bromfenvinphos-methyl6.0629510915109795
102.Heptachlor epoxide6.073532631326319329
103.Quinalphos6.07298156.18146.1118.110
104.Triadimenol6.07168.170.11012865.122
105.Triflumizole6.09205.917914179143.814
106.Captan6.101491056106.87912
107.Procymidone6.1128367.1282839610
108.Folpet6.14259.913016103.97610
109.Chlorbenside6.15268125.1812589.117
110.Bromophos-ethyl6.17358.930317330.93038
111.trans-Chlordane6.193752661827223712
112.Paclobutrazol6.19237.812710236.1125.112
113.2,4'-DDE6.193162461524617630
114.Tetrachlorvinphos6.203331091733110920
115.Fenamiphos6.25303.1195.182172029
116.Flutolanil6.262811731017314514
117.Prothiofos6.263092391526722116
118.cis-Chlordane6.273752661827223712
119.Bromfenvinphos6.273252691032326710
120.Fludioxonil6.2724812730153.81278
121.Flutriafol6.27219.112314123.19512
122.Iodofenphos6.273773323037736215
123.Pretilachlor6.27262202816213218
124.Profenofos6.273391883033726713
125.Chlorfenvinphos 26.273232671026715915
126.Endosulfan I6.28241206101951596
127.trans-Nonachlor6.284092632540930023
128.Chlorfenson6.2930217581751118
129.Oxadiazon6.33258175817511213
130.Oxyfluorfen6.3430022315252.1146.133
131.Myclobutanil6.38179125141791528
132.Bupirimate6.39316.2208.28273.1193.28
133.Flusilazole6.39233.1164.918206.113720
134.4,4'-DDE6.403162461524617630
135.Tricyclazole6.41189135.21818916212
136.2,4'-DDD6.42235165.121235199.116
137.Dieldrin6.42277241826319334
138.Fluazifop-P-butyl6.42383.1268.28383.1282.212
139.Chlorfenapyr6.46247227.1121377528
140.Ethylan6.462231671222319328
141.Nitrofen6.4928320210202139.120
142.Chlorthiophos 16.50256.916526256.923912
143.Chlorobenzilate6.522511391413911112
144.Endrin6.552631933024517325
145.Ethion6.58231129241539710
146.4,4'-DDD6.59235165.121235199.116
147.Chlorthiophos 26.61325269142972698
148.2,4'-DDT6.62235165.121235199.116
149.Triazophos6.65256.9161.78161134.18
150.cis-Nonachlor6.654092632540930023
151.Sulprofos6.66322156815614113
152.Carfentrazone ethyl6.67340.2312.210330310.18
153.Endrin aldehyde6.68344.9243.117344.9244.914
154.4,4'-Methoxychlor olefin6.70308223.130238.1152.135
155.Carbophenothion6.7034215710125976
156.Norflurazon6.74303145171459518
157.Edifenphos6.75310109291731098
158.Lenacil6.76153135.714135.852.918
159.4,4'-DDT6.61235165.121235199.116
160.Endosulfan sulfate6.81272237102412068
161.Hexazinone6.83171.171.1161288310
162.Piperonyl butoxide6.83176.110326176.1131.114
163.Propargite6.83201.181.110135.110714
164.Resmethrin6.83143.112810123.281.28
165.Tebuconazole6.85250.1125.2221258916
166.Nitralin6.95316.12748274216.26
167.Captafol6.99150.878.9187977.112
168.TPP (IS)6.993261693032621520
169.Iprodione7.0131424514187124.124
170.Bifenthrin7.05181.1166.110165.1115.130
171.Fenpropathrin7.05265210818115224
172.Pyridaphenthion7.05340.1199.18199.177.126
173.Tetramethrin7.06164772516410712
174.Bromopropylate7.08340.818315183154.912
175.Azinphos-ethyl7.8016077181327712
176.EPN7.1116977221691418
177.Phosmet7.11160772416013310
178.Methoxychlor7.122271413322716925
179.Tebufenpyrad7.12333276827617110
180.Endrin ketone7.13317101213152798
181.Phenothrin7.19183.1168.112123.281.18
182.Tetradifon7.252271991015913110
183.Pyriproxyfen7.28226.1186.116136.17820
184.Phosalone7.293671113618211114
185.Leptophos7.31377269371717718
186.λ-Cyhalothrin7.31197.1141.1101979126
187.Acrinathrin7.32289.193102899124
188.Pyrazophos7.41265.1210.110221.1193.110
189.Mirex7.442742391527223715
190.Fenarimol7.46219107.11213911116
191.Azinphos-methyl7.4616077181327712
192.Pyraclofos7.473601391419413818
193.cis-Permethrin7.54183.1153.112163127.16
194.trans-Permethrin7.58183.1153.112163127.16
195.Pyridaben7.62147117201471198
196.Coumaphos7.663621091721018210
197.Fluquinconazole7.663401084234029814
198.Prochloraz7.67308701318013812
199.Cyfluthrin7.73226.1199822615130
200.Cypermethrin7.83181.112728181.1152.120
201.Flucythrinate 17.86199.1157.18157.1107.113
202.Acequinocyl7.89342.4188.11418813210
203.Etofenprox7.90163.110718163.1135.110
204.Flucythrinate 27.91199.1157.18157.1107.113
205.Fluridone8.03328.1127.140328.125926
206.Fenvalerate8.10169.1127.110167.11258
207.Tau-fluvalinate8.152525517250.15523
208.Fenvalerate8.16169.1127.110167.11258
209.Deltamethrin8.33252.993.119181.115220
ColumnLow-pressure GC column kit (factory-coupled restrictor column [5 m x 0.18 mm ID] and Rtx-5ms analytical column [15 m, 0.53 mm ID, 1 µm plus 1 m integrated transfer line on the outlet end]) (cat.# 11800)
SampleGC multiresidue pesticide kit (cat.# 32562)
Triphenylphosphate (cat.# 33258)
Anthracene (cat.# 33264)
Diluent:Acetonitrile
Conc.:1 µg/mL
Injection
Inj. Vol.:1 µL splitless (hold 0.5 min)
Liner:Topaz 4.0 mm ID single taper inlet liner w/ wool (cat.# 23447)
Inj. Temp.:250 °C
Oven
Oven Temp.:80 °C (hold 1 min) to 320 °C at 35 °C/min (hold 5 min)
Carrier GasHe, constant flow
Flow Rate:2 mL/min
DetectorTSQ 8000
SIM Program:35-550 m/z
Transfer Line Temp.:290 °C
Analyzer Type:Quadrupole
Source Temp.:325 °C
Solvent Delay Time:2 min
Tune Type:PFTBA
Ionization Mode:EI
InstrumentThermo Scientific TSQ 8000 Triple Quadrupole GC-MS
NotesSample preparation: 10 g of homogenized strawberries were fortified with the internal standards at 20 ppb and then extracted with 10 mL of acetonitrile and QuEChERS EN 15662 salts (cat.# 25850). After centrifugation, 1 mL of supernatant was added to a 2 mL dSPE vial containing magnesium sulfate and PSA (cat.# 26124) for cleanup. The cleaned extract was spiked with GC multiresidue pesticide mix at 1 ppm.