Terpenes MegaMix #2 on Rxi-1301Sil MS

All compounds at 10 µg/mL.

Standard/Sample
Column	Rxi-1301Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 16094)
	Terpenes MegaMix #2 (cat.# 34143)

Diluent:	Isopropanol
Conc.:	10 µg/mL
Injection
Inj. Vol.:	1 µL split (split ratio 25:1)
Liner:	Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:	280 °C
Split Vent Flow Rate:	45 mL/min
Oven
Oven Temp.:	40 °C (hold 0.5 min) to 100 °C at 3 °C/min to 200 °C at 8 °C/min to 300 °C at 25 °C/min (hold 3 min)
Carrier Gas	He, constant flow
Flow Rate:	1.8 mL/min

Detector

5977B

Scan Program:

Group	Start Time (min)	Scan Range (amu)	Scan Rate (scans/sec)
1	6.5	35-350	2.3

Transfer Line Temp.:

300 °C

Analyzer Type:

Quadrupole

Source Type:

HES

Source Temp.:

325 °C

Quad Temp.:

200 °C

Electron Energy:

70 eV

Solvent Delay Time:

6.5 min

Tune Type:

BFB

Ionization Mode:

Instrument

Agilent 7890B GC & 5977B MSD

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