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Peaks | |
---|---|
1. | Acetone |
2. | Acrylonitrile |
3. | carbon disulfide impurity |
4. | Hexane |
5. | Methyl ethyl ketone |
6. | Ethyl acetate |
7. | Methyl Cellosolve® |
8. | Tetrahydrofuran |
9. | n-Butyl alcohol |
Peaks | |
---|---|
10. | Isopropyl acetate |
11. | Heptane |
12. | n-Propyl acetate |
13. | Amyl alcohol |
14. | Toluene |
15. | n-Butyl acetate |
16. | n-Butyl acrylate |
17. | Cellosolve® acetate |
18. | Cyclohexanone |
Column | Rtx-5, 60 m, 0.32 mm ID, 3.00 µm (cat.# 10287) |
---|---|
Standard/Sample | solvents collected on a charcoal tube and extracted in carbon disulfide |
Injection | |
Inj. Vol.: | 1.0 µL split |
Inj. Temp.: | 300 °C |
Oven | |
Oven Temp.: | 50 °C (hold 4 min) to 120 °C at 5 °C/min (hold 20 min) |
Carrier Gas | H2, constant pressure |
Linear Velocity: | 40 cm/sec @ 50 °C |
Detector | FID @ 300 °C |
---|---|
Notes | FID sensitivity: 128 x 10-12 AFS |
Acknowledgement | Permission to publish this chromatogram granted by Kenda McCoy, Rexham Industrial. |