Derivatized Amphetamines (500 ng/mL) on Rxi-5Sil MS

GC_CF1144

	Peaks
1.	Amphetamine
2.	Methamphetamine
3.	MDA
4.	MDMA
5.	MDEA

c = contaminant

Standard/Sample
Column	Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Diluent:	Butyl chloride
Conc.:	500 ng/mL HFAA derivatives
Injection
Inj. Vol.:	1 µL splitless (hold 1 min)
Liner:	3.5 mm splitless taper w/wool (cat.# 22286-200.1)
Inj. Temp.:	250 °C
Purge Flow:	28 mL/min
Oven
Oven Temp.:	75 °C to 300 °C at 15 °C/min
Carrier Gas	He, constant linear velocity
Linear Velocity:	45 cm/sec, 13.5 psi, 93.1 kPa @ 75 °C

Detector	MS
Mode:	Scan
Transfer Line Temp.:	250 °C
Analyzer Type:	Quadrupole
Source Temp.:	200 °C
Electron Energy:	70 eV
Solvent Delay Time:	4 min
Tune Type:	PFTBA
Ionization Mode:	EI
Scan Range:	40-300 amu
Scan Rate:	5 scans/sec
Instrument	Shimadzu 2010 GC & QP2010+ MS