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Semivolatiles SVOC MegaMix 100 Kit on Rxi-SVOCms

GC_EV1508
PeakstR (min)
1.N-Nitrosodimethylamine2.771
2.Pyridine2.839
3.Acrylamide3.789
4.Phenol5.169
5.Aniline5.281
6.Bis(2-chloroethyl) ether5.334
7.2-Chlorophenol5.449
8.Decane5.469
9.1,3-Dichlorobenzene5.668
10.1,4-Dichlorobenzene5.762
11.Benzyl alcohol5.879
12.1,2-Dichlorobenzene5.977
13.2-Methylphenol6.002
14.2,2'-Oxybis(1-chloropropane)6.072
15.Indene6.095
16.3-Methylphenol6.212
17.4-Methylphenol6.212
18.N-Nitroso-di-n-propylamine6.247
19.Hexachloroethane6.46
20.Nitrobenzene6.523
21.Isophorone6.855
22.2-Nitrophenol6.985
23.2,4-Dimethylphenol6.993
24.Benzoic acid7.061
25.O,O,O-Triethyl phosphorothioate7.102
26.Bis(2-chloroethoxy)methane7.149
27.2,4-Dichlorophenol7.326
28.1,2,4-Trichlorobenzene7.473
29.α-Terpineol7.597
30.Naphthalene7.597
31.4-Chloroaniline7.648
32.Hexachlorobutadiene7.771
33.Quinoline8.093
PeakstR (min)
34.4-Chloro-3-methylphenol8.344
35.2-Methylnaphthalene8.644
36.1-Methylnaphthalene8.798
37.Hexachlorocyclopentadiene8.881
38.2,3-Dichloroaniline9.059
39.2,4,6-Trichlorophenol9.059
40.2,4,5-Trichlorophenol9.107
41.2-Chloronaphthalene9.396
42.2-Nitroaniline9.526
43.1,2-Dinitrobenzene9.732
44.Dimethyl phthalate9.797
45.1,3-Dinitrobenzene9.847
46.2,6-Dinitrotoluene9.895
47.1,4-Dinitrobenzene9.978
48.Acenaphthylene10.044
49.3-Nitroaniline10.156
50.Acenaphthene10.312
51.2,4-Dinitrophenol10.312
52.4-Nitrophenol10.371
53.2,4-Dinitrotoluene10.52
54.Dibenzofuran10.577
55.2,3,5,6-Tetrachlorophenol10.683
56.2,3,4,6-Tetrachlorophenol10.75
57.Diethyl phthalate10.892
58.Hexadecane10.917
59.Zinophos11.021
60.4-Nitroaniline11.103
61.Fluorene11.105
62.4-Chlorophenyl phenyl ether11.105
63.4,6-Dinitro-2-methylphenol11.155
64.Diphenylamine11.269
65.Azobenzene11.343
66.Sulfotep11.494
PeakstR (min)
67.Phorate11.73
68.4-Bromophenyl phenyl ether11.86
69.Dimethoate11.976
70.Hexachlorobenzene11.976
71.Pentachlorophenol12.26
72.Octadecane12.355
73.Disulfoton12.542
74.Dinoseb12.542
75.Phenanthrene12.615
76.Anthracene12.695
77.Carbazole12.925
78.Methyl parathion13.128
79.di-n-Butyl phthalate13.438
80.Ethyl Parathion13.73
81.Fluoranthene14.472
82.Benzidine14.648
83.Pyrene14.832
84.Famphur15.739
85.Benzyl butyl phthalate15.838
86.Bis(2-ethylhexyl) adipate15.958
87.3,3'-Dichlorobenzidine16.922
88.4,4-Methylene-bis(2-chloroaniline)17.009
89.Benz[a]anthracene17.009
90.Di-n-octyl phthalate17.011
91.Chrysene17.092
92.6-Methylchrysene18.212
93.Bis(2-ethylhexyl) phthalate18.744
94.Benzo[b]fluoranthene19.953
95.Benzo[k]fluoranthene20.043
96.Benzo[a]pyrene21.06
97.Dibenz(a,h)acridine24.633
98.Indeno[1,2,3-cd]pyrene25.607
99.Dibenz[a,h]anthracene25.739
100.Benzo[ghi]perylene26.795
ColumnRxi-SVOCms, 30 m, 0.25 mm ID, 0.50 µm (cat.# 16638)
Standard/SampleSVOC MegaMix 100 kit (cat.# 31908)
Diluent:Dichloromethane
Conc.:20 µg/mL (2 ng on-column)
Injection
Inj. Vol.:1 µL split (split ratio 10:1)
Liner:Topaz 4.0 mm ID single taper inlet liner w/ wool (cat.# 23303)
Inj. Temp.:250 °C
Oven
Oven Temp.:60 °C (hold 1 min) to 285 °C at 16 °C/min to 305 °C at 1.65 °C/min to 330 °C at 8.8 °C/min (hold 4.55 min)
Carrier GasHe, constant flow
Flow Rate:1.2 mL/min
DetectorMS
Mode:Scan
Scan Program:
GroupStart Time
(min)		Scan Range
(amu)		Scan Rate
(scans/sec)
12.050-5003.6
Transfer Line Temp.:280 °C
Analyzer Type:Quadrupole
Source Type:Inert
Drawout Plate:6 mm ID
Source Temp.:330 °C
Quad Temp.:180 °C
Electron Energy:70 eV
Solvent Delay Time:2 min
Tune Type:DFTPP
Ionization Mode:EI
InstrumentAgilent 7890A GC & 5975C MSD
Sample PreparationSolutions were mixed and diluted to 20 ppm with dichloromethane in amber 2 mL, 9 mm short-cap, screw-thread vials (cat.# 21143) and sealed with 2.0 mL, 9 mm short-cap, screw-vial closures (cat.# 23842).
NotesThe SVOC MegaMix 100 kit (cat.# 31908) contains one ampul each of the following standards.
• 8270 MegaMix (cat.# 31850)
• SVOC Additions standard (cat.# 31909)
• Benzoic acid (cat.# 31879)
AcknowledgementChris Rattray
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