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Rosemary Oil on Rt-βDEXsm

GC_FF1355
PeakstR1tR2
1.α-Pinene (±)10.50010.941
2.Camphene (±)11.56611.952
3.β-Pinene (±)12.69013.200
4.Limonene (±)14.85015.585
5.Eucalyptol (1,8-cineole)15.837-
PeakstR1tR2
6.Linalool (±)26.01126.463
7.Camphor (±)27.49227.704
8.Terpinen-4-ol (±)30.64730.935
9.Isoborneol (±)32.25432.786
10.Borneol (±)33.00033.756
11.α-Terpineol (±)33.53934.237
ColumnRt-βDEXsm, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13104)
Standard/SampleRosemary oil
Diluent:Acetone
Conc.:5%
Injection
Inj. Vol.:1 µL split (split ratio 100:1)
Liner:Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305)
Inj. Temp.:210 °C
Oven
Oven Temp.:40 °C (hold 1 min) to 200 °C at 2 °C/min (hold 3 min)
Carrier GasH2, constant pressure
Linear Velocity:80 cm/sec
DetectorFID @ 230 °C
Constant Column + Constant Make-up:51.4 mL/min
Make-up Gas Type:N2
Data Rate:50 Hz
InstrumentAgilent 7890A GC
Sample PreparationRosemary oil (50 µL) was diluted with acetone (950 µL) in 2 mL, screw-thread vials (cat.# 21143), and capped with short-cap, screw-vial closures (cat.# 24495).