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Peaks | tR 1 | tR 2 | |
---|---|---|---|
1. | Eucalyptol | 13.825 | - |
2. | Limonene (L,D) | 17.898 | 18.886 |
3. | Linalool oxides | 21.210 | 21.638 |
4. | Camphor | 24.357 | - |
5. | Linalool (±) | 25.688 | 26.651 |
6. | Linalyl acetate | 29.166 | 29.494 |
Column | Rt-βDEXse, 30 m, 0.32 mm ID, 0.25 µm (cat.# 13106) |
---|---|
Standard/Sample | Lavender oil |
Diluent: | Acetone |
Conc.: | 5% |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 100:1) |
Liner: | Topaz 4.0 mm ID Precision inlet liner w/ wool (cat.# 23305) |
Inj. Temp.: | 210 °C |
Oven | |
Oven Temp.: | 40 °C (hold 1 min) to 230 °C at 2 °C/min (hold 3 min) |
Carrier Gas | H2, constant flow |
Linear Velocity: | 80 cm/sec @ 40 °C |
Detector | FID @ 230 °C |
---|---|
Constant Column + Constant Make-up: | 51.4 mL/min |
Make-up Gas Type: | N2 |
Hydrogen flow: | 40 mL/min |
Air flow: | 400 mL/min |
Data Rate: | 50 Hz |
Instrument | Agilent 7890A GC |
Sample Preparation | Lavender oil (50 µL) was diluted with acetone (950 µL) in 2 mL, screw-thread vials (cat.# 21143), and capped with short-cap, screw-vial closures (cat.# 24495). |