Residual Pesticides Analysis of Botanical Ingredients Using Gas Chromatography Triple Quadrupole Mass Spectrometry

Author(s): Riki Kitano1, Tairo Ogura1, Nicole Lock1, Robert Clifford1, Julie Kowalski2, Jack Cochran2, Dan Li2
1. Shimadzu Scientific Instruments, Inc. 2. Restek Corporation

Published By: Restek Corporation

Year of Publication: 2019

Link: www.restek.com/Technical-Resources/Technical-Library/Foods-Flavors-Fragrances/fff_FSAR3080-UNV

Abstract: Dietary supplements, which are consumed worldwide, are made from various botanical ingredients. To be safe from pesticides exposure, residual pesticides must be monitored by chromatographic instrumentation. Issues arise, however, due to the fact these botanical samples are dried and cause large interferences in the chromatography. This study shows that the modified QuEChERS method combined with GC-MS/MS achieves consistent pesticides monitoring in botanical ingredients.

Acknowledgment(s): Originally published by Shimadzu Corporation in collaboration with Restek Corporation.

Cannabidivarin (CBDV) Added to Restek’s Selection of Cannabis Reference Standards

Cannabis strains with high levels of cannabidiol (CBD) typically have higher levels of cannabidivarin (CBDV) as well, but accurate quantitation of both compounds for potency and strain ID is a must, especially as interest in using CBDV as an anticonvulsant and anti-nausea treatment continues to rise. Restek now offers a stand-alone CBDV reference standard—in addition to CBD and a host of other compounds—to help labs with the comprehensive analysis of cannabis products.

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New Pesticide CRMs Released Specifically for Cannabis Labs in California and Similar States

Restek’s support for cannabis-testing labs continues to grow. This latest offering will help you meet the specific cannabis analysis needs of California set forth by the Bureau of Cannabis Control for regulated category I and II residual pesticide reporting—and of other states with similar regulations/programs. Ideal for creating multipoint (5-point minimum suggested) calibration curves for GC- and LC-MS/MS, these six mixes of prepared stock standards also eliminate the need for in-house standards preparation. And, as with all certified reference materials (CRMs) manufactured and QC tested in Restek’s ISO-accredited labs, they will satisfy your ISO requirements.

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