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Column | Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623) |
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Standard/Sample | |
Diluent: | Ethyl acetate |
Conc.: | 50 ng/mL TMS derivatives |
Injection | |
Inj. Vol.: | 1 µL splitless (hold 1 min) |
Liner: | 3.5 mm splitless taper w/wool (cat.# 22286-200.1) |
Inj. Temp.: | 250 °C |
Purge Flow: | 21.4 mL/min |
Oven | |
Oven Temp.: | 150 °C to 330 °C at 15 °C/min (hold 3 min) |
Carrier Gas | He, constant linear velocity |
Linear Velocity: | 40 cm/sec, 13.8 psi, 95.1 kPa @ 150 °C |
Detector | MS | |
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Mode: | SIM | |
SIM Program: | 390, 337, 458, 367, 382, 310, 371, 386, 343, 473, 398 m/z | |
Transfer Line Temp.: | 280 °C | |
Analyzer Type: | Quadrupole | |
Source Temp.: | 200 °C | |
Solvent Delay Time: | 4 min | |
Tune Type: | PFTBA | |
Ionization Mode: | EI | |
Instrument | Shimadzu 2010 GC & QP2010+ MS |
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