Derivatized Cannabinoids (50 ng/mL) on Rxi-5Sil MS

GC_CF1146

Standard/Sample
Column	Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Diluent:	Ethyl acetate
Conc.:	50 ng/mL TMS derivatives
Injection
Inj. Vol.:	1 µL splitless (hold 1 min)
Liner:	3.5 mm splitless taper w/wool (cat.# 22286-200.1)
Inj. Temp.:	250 °C
Purge Flow:	21.4 mL/min
Oven
Oven Temp.:	150 °C to 330 °C at 15 °C/min (hold 3 min)
Carrier Gas	He, constant linear velocity
Linear Velocity:	40 cm/sec, 13.8 psi, 95.1 kPa @ 150 °C

Detector	MS
Mode:	SIM
SIM Program:	390, 337, 458, 367, 382, 310, 371, 386, 343, 473, 398 m/z
Transfer Line Temp.:	280 °C
Analyzer Type:	Quadrupole
Source Temp.:	200 °C
Solvent Delay Time:	4 min
Tune Type:	PFTBA
Ionization Mode:	EI
Instrument	Shimadzu 2010 GC & QP2010+ MS

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