Derivatized Amphetamines (50 ng/mL) on Rxi-5Sil MS

	Peaks	m/z 1	m/z 2	m/z 3
1.	Amphetamine	118	240	91
2.	Methamphetamine	254	118	91
3.	MDA	135	162	240
4.	MDMA	254	162	135
5.	MDEA	268	240	162

c = contaminant

Standard/Sample
Column	Rxi-5Sil MS, 30 m, 0.25 mm ID, 0.25 µm (cat.# 13623)
Diluent:	Butyl chloride
Conc.:	50 ng/mL HFAA derivatives
Injection
Inj. Vol.:	1 µL splitless (hold 1 min)
Liner:	3.5mm Gooseneck Splitless w/Wool (cat.# 22286-200.1)
Inj. Temp.:	250 °C
Purge Flow:	28.8 mL/min
Oven
Oven Temp.:	75 °C to 300 °C at 15 °C/min
Carrier Gas	He, constant linear velocity
Linear Velocity:	45 cm/sec, 13.5 psi, 93.1 kPa @ 75 °C

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