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Peaks | |
---|---|
1. | Diethylamine |
2. | Pyridine |
3. | Morpholine |
4. | Phenol |
5. | Aniline |
6. | 2-Chlorophenol |
Peaks | |
---|---|
7. | Diethylenetriamine |
8. | Octylamine |
9. | 1-Methyl-2-Pyrrolidinone |
10. | 2-Nitrophenol |
11. | 2,6-Dimethylaniline |
12. | Nicotine |
13. | 2-Nitroaniline |
Column | Rtx-5 Amine, 30 m, 0.32 mm ID, 1.00 µm (cat.# 12354) |
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Standard/Sample | amines and phenols |
Diluent: | water |
Conc.: | 22 ng on-column |
Injection | |
Inj. Vol.: | 1 µL split (split ratio 25:1) |
Inj. Temp.: | 305 °C |
Oven | |
Oven Temp.: | 120 °C to 220 °C at 10 °C/min |
Carrier Gas | H2, constant pressure |
Linear Velocity: | 38 cm/sec @ 120 °C |
Detector | FID @ 305 °C |
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Notes | FID sensitivity: 6.4 x 10-11 AFS |