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Peaks | |
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1. | Dichlorvos |
2. | Hexamethylphosphoramide |
3. | Mevinphos |
4. | Trichlorfon |
5. | TEPP |
6. | Thionazin (IS) |
7. | Demeton-o |
8. | Ethoprop |
9. | Tributyl phosphate (SS) |
10. | Dicrotophos |
11. | Monocrotophos |
12. | Naled |
13. | Sulfotepp |
14. | Phorate |
15. | Dimethoate |
16. | Demeton-S |
17. | Dioxathion |
Peaks | |
---|---|
18. | Terbufos |
19. | Fonophos |
20. | Phosphamidon isomer |
21. | Diazinon |
22. | Disulfoton |
23. | Phosphamidon |
24. | Dichlorofenthion |
25. | Methyl parathion |
26. | Chlorpyrifos methyl |
27. | Ronnel |
28. | Fenitrothion |
29. | Malathion |
30. | Fenthion |
31. | Aspon |
32. | Parathion-ethyl |
33. | Chlorpyrifos |
34. | Trichloronate |
Peaks | |
---|---|
35. | Chlorfenvinphos |
36. | Merphos |
37. | Crotoxyphos |
38. | Stirofos |
39. | Prothiofos |
40. | merphos oxidation product |
41. | Fensulfothion |
42. | Famphur |
43. | Ethion |
44. | Sulprofos |
45. | Carbophenothion |
46. | Triphenyl phosphate (IS) |
47. | Phosmet |
48. | EPN |
49. | Azinphos-methyl |
50. | Leptophos |
51. | Tri-o-cresyl phosphate |
52. | Azinphos-ethyl |
53. | Coumaphos |
Column | Rtx-1, 30 m, 0.32 mm ID, 0.50 µm (cat.# 10139) |
---|---|
Standard/Sample | Triphenylphosphate (cat.# 32281) |
Tributylphosphate (cat.# 32280) | |
8140/8141 OP Pesticide Calibration Mix A (cat.# 32277) | |
8141 OP Pesticide Calibration Mix B (cat.# 32278) | |
Diluent: | Hexane |
Conc.: | Total OPP custom standard mix (0.2µg/mL), 1µL US EPA Method 8141A custom standard mixes (200ng/mL) |
Injection | splitless (hold 1.0 min) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 100 °C to 180 °C at 10 °C/min (hold 2 min) to 300 °C at 18 °C/min (hold 3 min) |
Dead Time: | 0.78 min @ 100 °C |
Detector | FPD @ 280 °C |
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