Organophosphorus Pesticides (European) on Rtx-CLPesticides

Injection
Column	Rtx-CLPesticides, 30 m, 0.25 mm ID, 0.25 µm (cat.# 11123)
Sample	Custom European Mix
	1-Bromo-2-nitrobenzene (cat.# 32279)
	4-Chloro-3-nitrobenzotrifluoride (cat.# 32282)
	Tributylphosphate (cat.# 32280)
	Triphenylphosphate (cat.# 32281)
Inj. Vol.:	1.0 µL splitless (hold 0.4 min)
Liner:	Double Gooseneck Splitless (4mm) (cat.# 20785)
Inj. Temp.:	250 °C
Oven
Oven Temp.:	80 °C (hold 1.0 min) to 150 °C at 7 °C/min to 280 °C at 15 °C/min (hold 7 min)
Carrier Gas	He, constant flow
Flow Rate:	0.75 mL/min
Linear Velocity:	28 cm/sec
Dead Time:	1.82 min @ 80 °C

Detector	MS
Mode:	Scan
Transfer Line Temp.:	280 °C
Solvent Delay Time:	5 min
Tune Type:	PFTBA
Ionization Mode:	EI
Scan Range:	35-400 amu
Instrument	Agilent 5971A GC/MS
Notes	Carrier gas @ 6 psi head pressure

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