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Column | Rtx-5, 15 m, 0.25 mm ID, 0.25 µm (cat.# 10220) |
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Standard/Sample | motor oil composite (cat.# 31464) |
Diluent: | methylene chloride |
Conc.: | 500 µg/mL |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.5 min) |
Liner: | 4mm Splitless (cat.# 20904) |
Inj. Temp.: | 260 °C |
Oven | |
Oven Temp.: | 100 °C (hold 1 min) to 330 °C at 60 °C/min (hold 4 min) |
Carrier Gas | He, constant pressure |
Linear Velocity: | 76 cm/sec @ 50 °C |
Detector | FID @ 330 °C |
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Notes | oven using GC Racer |
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