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Organophosphorus Pesticides US EPA Method 8140/8141/8141A on Rtx-35

ColumnRtx-35, 30 m, 0.32 mm ID, 0.25 µm (cat.# 10424)
Standard/Sampletriphenylphosphate (cat.# 32281)
tributylphosphate (cat.# 32280)
8140/8141 OP Pesticide Calibration Mix A (cat.# 32277)
8141 OP Pesticide Calibration Mix B (cat.# 32278)
Conc.: 0.1µg/mL US EPA Method 8141A Custom Standard Mixes (100ng/mL)
Injection
Inj. Vol.:0.5 µL splitless (hold 5 min)
Liner:Drilled Uniliner (hole near top) (cat.# 21054-214.1)
Inj. Temp.:220 °C
Oven
Oven Temp.:100 °C to 180 °C at 10 °C/min (hold 2 min) to 300 °C at 18 °C/min (hold 10 min)
Carrier GasHe, constant pressure
Linear Velocity:42 cm/sec @ 60 °C
DetectorFPD @ 280 °C