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Peaks | |
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1. | 2,4,5,6 Tetrachloro-m-xylene (SS) |
2. | α-BHC |
3. | γ-BHC |
4. | β-BHC |
5. | δ-BHC |
6. | Heptachlor |
7. | Aldrin |
8. | Heptachlor epoxide |
9. | γ-Chlordane |
10. | α-Chlordane |
11. | 4,4'-DDE |
Peaks | |
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12. | Endosulfan I |
13. | Dieldrin |
14. | Endrin |
15. | 4,4'-DDD |
16. | Endosulfan II |
17. | 4,4'-DDT |
18. | Endrin aldehyde |
19. | Methoxychlor |
20. | Endosulfan sulfate |
21. | Endrin ketone |
22. | Decachlorobiphenyl (SS) |
Columns | Rtx-CLPesticides 30 m, 0.32 mm ID, 0.50 µm (cat.# 11139) |
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and Rtx-CLPesticides2 30 m, 0.32 mm ID, 0.25 µm (cat.# 11324) | |
using Siltek Guard Column .15 m, 0.32 mm ID (cat.# 10027) | |
with Universal Angled “Y” Press-Tight Connector (cat.# 20403) | |
Standard/Sample | Organochlorine Pesticide Mix AB #2 (cat.# 32292) |
2,4,5,6-tetrachloro-m-xylene (cat.# 32027) | |
decachlorobiphenyl (BZ #209) (cat.# 32029) | |
Diluent: | hexane |
Conc.: | Organochlorine Pesticide Mix AB #2 (cat.# 32292) 80/160/800 ppb, 2,4,5,6 tetrachloro- m-xylene (SS, cat.# 32027), 80ppb, decachlorobiphenyl (SS, cat.# 32029), 160ppb in hexane |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 0.75 min) |
Liner: | Drilled Uniliner (hole near top) (cat.# 21054) |
Inj. Temp.: | 210 °C |
Oven | |
Oven Temp.: | 110 °C (hold 1 min) to 245 °C at 20 °C/min to 300 °C at 6 °C/min |
Carrier Gas | H2, constant pressure |
Linear Velocity: | 60 cm/sec @ 300 °C |
Detector | ECD @ 310 °C |
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