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Peaks | |
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1. | 2,4,5,6-Tetrachloro-m-xylene |
2. | α-BHC |
3. | γ-BHC |
4. | β-BHC |
5. | δ-BHC |
6. | Heptachlor |
7. | Aldrin |
8. | Heptachlor epoxide |
9. | γ-Chlordane |
10. | α-Chlordane |
11. | Endosulfan I |
Peaks | |
---|---|
12. | 4,4'-DDE |
13. | Dieldrin |
14. | Endrin |
15. | 4,4'-DDD |
16. | Endosulfan II |
17. | Endrin aldehyde |
18. | 4,4'-DDT |
19. | Endosulfan sulfate |
20. | Methoxychlor |
21. | Endrin ketone |
22. | Decachlorobiphenyl |
Column | Rtx-440, 30 m, 0.32 mm ID, 0.50 µm (cat.# 12939) |
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Standard/Sample | Organochlorine Pesticide Mix AB #1 (cat.# 32291) |
Pesticide Surrogate Mix, EPA 8080, 8081 (cat.# 32000) | |
Diluent: | hexane |
Conc.: | 50 ng/mL each component |
Injection | |
Inj. Vol.: | 1.0 µL splitless (hold 1.0 min) |
Liner: | 3.5 mm Single Gooseneck (cat.# 20962) |
Inj. Temp.: | 250 °C |
Oven | |
Oven Temp.: | 110 °C (hold 0.5 min) to 268 °C at 30 °C/min to 290 °C at 11 °C/min to 320 °C at 25 °C/min (hold 5 min) |
Carrier Gas | H2, constant pressure |
Linear Velocity: | 71 cm/sec @ 110 °C |
Detector | ECD @ 310 °C |
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